ORIGINAL_ARTICLE
One-pot Synthesis of New Category of 2-aryl-quinazolinones Using of DSDABCO as an Efficient Heterocyclic Medium
A series of 2-aryl-quinazolin-4(1H)-ones have been synthesized in short reaction times and excellent yields through one-pot reaction between isatoic anhydride, glycine and various aldehydes in the presence of DSDABCO (1,4-disulfo-1,4-diazoniabicyclo[2.2.2] octane chloride) as an efficient heterocyclic ionic liquid media at room temperature. This method offers many advantages such as green environment, mild conditions, excellent efficiency, simple method and reduction of environmental consequences. Using recyclable ionic liquid and no need to another solvent or catalyst is an important step in green chemistry. On the other hand, this method does not require heating and is done at room temperature. The ionic liquid was recovered and reused. To the best of our knowledge, this is the first report for the synthesis of a new library of quinazolin-4(1H)-ones derived from glycine as a natural substrate based on green chemistry conditions. The structures of 2-aryl-quinazolin-4(1H)-ones were confirmed by 1H, 13CNMR, HRMS and FTIR spectral data and elemental analyses.
https://pccc.icrc.ac.ir/article_81728_c5f0fc7ac4a3cc17298d52e197d910df.pdf
2021-11-01
233
240
10.30509/pccc.2020.166733.1089
one-pot reaction
2-aryl-quinazolin-4(1H)-one
glycine
Ionic Liquid
A.
Keyhani
ar.keyhani@mail.com
1
Department of Chemistry, Islamic Azad University, Rasht Branch, Rasht, Iran.
AUTHOR
M.
Nikpassand
nikpassand@iaurasht.ac.ir
2
Department of Chemistry, Islamic Azad University, Rasht Branch, Rasht, Iran.
LEAD_AUTHOR
L.
Zare Fekri
chem_zare@yahoo.com
3
Department of Chemistry, Payame Noor University, Tehran, Iran.
AUTHOR
H.
Kefayati
kefayati@iaurasht.ac.ir
4
Department of Chemistry, Islamic Azad University, Rasht Branch, Rasht, Iran.
AUTHOR
M. Narasimhulu, Lee, Y. R. Ethylenediamine diacetate-catalyzed three-component reaction for the synthesis of 2, 3-dihydroquinazolin-4(1H)-ones and their spirooxindole derivatives, Tetrahedron, 67(2011), 9627-6934.
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H. R. Shaterian, A. R. Oveisi, PPA-SiO2 as a Heterogeneous Catalyst for Efficient Synthesis of 2‐Substituted‐1,2,3,4‐tetrahydro‐4‐quinazolinones under Solvent‐free Conditions, Chin. J. Chem., 27(2009), 2418-2422.
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Y. Yu, J. M. Ostresh, R. A. Houghten, A Traceless Approach for the Parallel Solid-Phase Synthesis of 2-(Arylamino)quinazolinones, J. Org. Chem., 67(2002), 5831-5834.
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8
M. Baghbanzadeh, P. Salehi, M. Dabiri, G. Kozehgary, Water-Accelerated Synthesis of Novel Bis-2,3-dihydroquinazolin-4(1H)-one Derivatives, Synthesis, (2006), 344-348.
9
M. Dabiri, P. Salehi, M. Baghbanzadeh, M. A. Zolfigol, M. Agheb, S. Heydari, Silica sulfuric acid: An efficient reusable heterogeneous catalyst for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones in water and under solvent-free conditions, Catal. Commun., 9(2008), 785-788.
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J. X. Chen, W. K. Su, H. Y. Wu, M. C. Liu, C. Jin, Eco-friendly synthesis of 2,3-dihydroquinazolin-4(1H)-ones in ionic liquids or ionic liquid–water without additional catalyst, Green Chem., 9(2007), 972-975.
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N. B. Darvatkar, S. V. Bhilare, A. R. Deorukhkar, D. G. Raut, M. M. Salunkhe, [bmim]HSO4: an efficient and reusable catalyst for one-pot three-component synthesis of 2,3-dihydro-4(1H)-quinazolinones, Green Chem. Lett. Rev., 3(2010), 301-306.
13
H. R. Shaterian, A. R. Oveisi, M. Honarmand, M. Synthesis of 2,3-Dihydroquinazoline-4(1H)-ones, Synth. Commun., 40(2010), 1231-1242.
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P. Salehi, M. Dabiri, M. Baghbanzadeh, M. Bahramnejad, One‐Pot, Three‐Component Synthesis of 2,3‐Dihydro‐4(1H)‐quinazolinones by Montmorillonite K‐10 as an Efficient and Reusable Catalyst, Synth. Commun., 36(2006), 2287-2292.
16
M. P. Surpur, P. R. Singh, S. B. Patil, S. D. Samant, Expeditious One‐Pot and Solvent‐Free Synthesis of Dihydroquinazolin‐4(1H)‐ones in the Presence of Microwaves, Synth. Commun., 37(2007), 1965-1970.
17
M. Z. Kassaee, S. Rostamizadeh, N. Shadjou, E. Motamedi, M. Esmaeelzadeh, An efficient one‐pot solvent‐free synthesis of 2,3‐dihydroquinazoline‐4(1H)‐ones via Al/Al2O3 nanoparticles, J. Heterocycl. Chem., 47(2010), 1421-1424.
18
Z. H. Zhang, H. Y. Lu, S. H. Yang, J. W. Gao, Synthesis of 2,3-dihydroquinazolin-4(1H)-ones by Three-Component Coupling of Isatoic Anhydride, Amines, and Aldehydes Catalyzed by Magnetic Fe3O4 Nanoparticles in Water, J. Comb. Chem., 12(2010), 643-646.
19
A. Saffar-Teluri, S. Bolouk, One-pot, three-component synthesis of 2,3-dihydroquinazolin-4(1H)-ones using p-toluenesulfonic acid–paraformaldehyde copolymer as an efficient and reusable catalyst, Monatsh. Chem., 141(2010), 1113-1115.
20
S. Rostamizadeh, A. M. Amani, G. H. Mahdavinia, H. Sepehrian, S. Ebrahimi, Synthesis of Some Novel 2-Aryl-Substituted 2,3-Dihydroquinazolin-4(1H)-ones under Solvent-Free Conditions Using MCM-41-SO3H as a Highly Efficient Sulfonic Acid, Synthesis, (2010), 1356-1360.
21
M. Mamaghani, K. Tabatabaeian, M. Mirzaeinejad, M. Nikpassand, One-pot facile conversion of Baylis-Hillman adducts into 1, 5-diarylpyrazoles using microwave irradiation, J. Iran. Chem. Soc., 3(2006), 89-92.
22
M. Nikpassand, L. Zare Fekri, M. Gharib, O. Marvi, Fe+3-montmorillonite K-10 as a Green and Reusable Catalyst for the Synthesis of New Generation of Dihydropyrimidinones, Lett. Org. Chem., 9(2012), 745-748.
23
M. Nikpassand, L. Zare Fekri, S. P. Helmi, DFT study of structure of azo-linked 4H-pyran dyes, J. Color Sci. Technol., 12(2018), 45-56
24
L. Zare Fekri M. Nikpassand, Synthesis of azo-linked bis coumarinyl methanes using [DBU] OAc ionic liquid at room temperature, J. Color Sci. Tech., 11(2017), 137-143.
25
M. Nikpassand, D. Pirdelzendeh, Green synthesis of novel azo-linked 2-phenyl benzimidazoles using ionic liquid [BDBIMm]Br, Dyes Pigm., 130(2016), 314-318.
26
M. Moayeri, M. Nikpassand, DFT study of aromatization on azo-linked cyclopentadienides, Prog. Color Colorants Coat., 14(2021), 13-26.
27
M. Nikpassand, L. Zare Fekri, K. Faraji Sina, S. Ziafatdoust Abed, O. Marvi, 3,3′-(butane-1,4-diyl) bis (1,2-dimethyl-1H-imidazol-3-ium)dibromide [BDBIm]Br-An efficient reusable ionic liquid for the microwave-assisted synthesis of quinazolinones, Russ. J. General Chem., 85(2015), 1959-1964.
28
L. Zare Fekri, M. Nikpassand, R. Maleki, 1, 4-Diazabicyclo[2.2.2]octanium diacetate: As an effective, new and reusable catalyst for the synthesis of benzo [d] imidazole, J. Mol. Liq., 222(2016), 77-81.
29
A. Masoumi Shahi, M. Nikpassand, L. Zare Fekri, An efficient and green synthesis of new benzo[f]chromenes using 1,4-disulfo-1,4-diazoniabicyclo[2.2.2]octane chloride as a novel medium
30
ORIGINAL_ARTICLE
Dyeing of Shoe Upper Leather with Extracted Dye from Acacia Nilotica Plant Bark-An Eco-Friendly Initiative
In recent years, the application of non-toxic and eco-friendly natural dyes for textile and leather coloration is getting interest among manufacturers and buyers due to the hazardous impact of conventional azo dyes. Natural dyes have extensive use in textiles, yet their application to leather is very limited. In this research, the prospect of using dye extracted from Acacia nilotica bark for dyeing of shoe upper leather was examined. Chrome-tanned goatskins were employed as raw material for dyeing with the extracted dye using drum dyeing method. The dyeing process was conducted with and without mordant, following pre-mordanting and post-mordanting techniques. Color analysis, various colorfastness tests, and determination of dye exhaustion rate were conducted to evaluate the dyeing quality. It was observed that the experimental dye imparted amber color to the leather that turned brown and gray upon mordanting with potash alum and ferrous sulfate, respectively. The dyed leather samples showed excellent colorfastness but moderate heat and light fastnesses. Mordanted dyed samples, especially the prr-mordanted dyed samples, possessed a better color intensity and more dye exhaustion rate. The leather samples dyed with extracted dye also increased the strength property of the leather and various color shades were produced by mordanting techniques.
https://pccc.icrc.ac.ir/article_81727_709f577b32c7ca2e8848f144ac133608.pdf
2020-11-01
241
258
10.30509/pccc.2020.166673.1074
Leather
Natural Dye
Acacia nilotica
Colorfastness
Eco-friendly
M. M.
Mahdi
miz40.mahdi@gmail.com
1
Department of Leather Engineering, Institute of Leather Engineering and Technology, University of Dhaka, Dhaka, Bangladesh
AUTHOR
F.
Tuj-Zohra
fatema.ilet@du.ac.bd
2
Department of Leather Products Engineering, Institute of Leather Engineering and Technology, University of Dhaka, Dhaka, Bangladesh
AUTHOR
S.
Ahmed
soburahmed@du.ac.bd
3
Department of Leather Engineering, Institute of Leather Engineering and Technology, University of Dhaka, Dhaka, Bangladesh
LEAD_AUTHOR
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126
ORIGINAL_ARTICLE
The Effect of Zn (II) Containing Metal-Organic Frameworks on Perovskite Solar Cells
In this study, we use metal-organic frameworks (MOFs), TMU-60 ([Zn (OBA)(L*). DMF]L*=5,6-di(pyridine-4-yl)-1,2,3,4 – tetrahydropyrazine) (compound I), and TMU-60-Cd (compound II), with excellent conductivity as additives in perovskite solution. The presence of cadmium in the structure of TMU-60-Cd can significantly enhance the conductivity of the framework. These frameworks can transfer the electron between the structures. Therefore, the use of these frameworks in perovskite solar cells could have a positive effect on electron transfer. However due to the creation of a lot of voids during the formation of perovskite layer, the power-conversion efficiency (PCE) of resulting PCSs were weaker than the pristine PCS. The results revealed that using even small amounts of TMU-60, and TMU-60-Cd caused a significant reduction in PCE, and the short current densities (Jsc), while improving the stability of the perovskite film, and the device. The absorption, and morphology of the new perovskite layer was also studied by UV–Vis spectroscopy, FE-SEM, and XRD.
https://pccc.icrc.ac.ir/article_81729_691b4086474c5bdc120336a5736869c0.pdf
2020-11-21
259
267
10.30509/pccc.2020.166700.1081
Metal-organic framework
TMU-60
TMU-60-Cd
Perovskite
Solar cells
Additive
M.
Seifpanah Sowmehesaraee
mahseiff@gmail.com
1
Department of Chemical Technologies, Iranian Research Organization for Science and Technology (IROST), Tehran, Iran
AUTHOR
M.
Ranjbar
marandjbar@irost.ir
2
Department of Chemical Technologies, Iranian Research Organization for Science and Technology (IROST), Tehran, Iran
LEAD_AUTHOR
M.
Abedi
mabedi@irost.ir
3
Department of Chemical Technologies, Iranian Research Organization for Science and Technology (IROST), Tehran, Iran
LEAD_AUTHOR
F.
Rouhani
rouhani_farzaneh@yahoo.com
4
Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, Tehran, Iran
AUTHOR
A.
Morsali
morsali_a@yahoo.com
5
Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, Tehran, Iran
AUTHOR
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2
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35
ORIGINAL_ARTICLE
Impact Strength of the Ni-P Coated Spring Steel with Varied Phosphate Content and Notch Orientation
Spring steel is a prominent piece of material in the automotive, aerospace and marine engineering applications. The existence of crack like flaws cannot be precluded in any engineering structures. During the course of manufacturing or under service conditions, corner cracks are formed. In the present experimental investigation, the impact toughness of spring steel with flat and corner notches has been analyzed. Also, the surface roughness and micro hardness studies have been carried out. The samples were coated with electroless Ni-P coating with varied phosphate content from 5 to 15%. The specimen preparation and the experimentations have been carried out according to the ASTM standards. Low velocity pendulum impact testing has been adopted for the experimentation with the corner notched specimen placed diagonally in the anvil. Results have revealed that the face notched sample has lower impact toughness compared to the corner notched one. The micromechanism study has shown that, even though the impact toughness of the corner notched samples is high, their failure behavior is more dangerous and unpredictable. The Ni-P coating with 10 % phosphate showed high impact toughness and delayed fracture.
https://pccc.icrc.ac.ir/article_81742_607fa2c8192dc5788a1faae80d85a825.pdf
2021-11-01
269
280
10.30509/pccc.2021.166701.1082
Impact strength
electroless Ni-P coating
Corner Notch
SEM
bonding strength
S.
Manjula
manjulasathish21@gmail.com
1
Department of Mechanical Engineering, Government Engineering College, Hassan, Karnataka, India.
AUTHOR
K. V.
Arun
bdt.arun@gmail.com
2
Department of Mechanical Engineering, Government Engineering College, HaveriKarnataka, India.
LEAD_AUTHOR
J. G. Mercer, T. Nicholas, Growth of short cracks in a notch plastic zone, Int. J. Fatigue.,13(1991), 263-270.
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23
ORIGINAL_ARTICLE
Hydrogen-free Cu: Amorphous-C: N Coating on TC4 Titanium Alloy: The Role of Gas Ratio on Mechanical and Antibacterial Potency
Ti-6Al-4V alloy, also called TC4, substrates are sputter-deposited by Cu: amorphous-C: N (Cu:a-C:N) thin coatings using planar magnetron sputtering physical vapor deposition device. Mixtures of argon and nitrogen at different ratios are selected as the sputtering atmosphere, and no hydrocarbon gas is used. Correlation of microstructure, morphology, surface properties, antibacterial characteristics, and mechanical performance of the coatings to the N2/Ar ratio are discussed. The outcomes from Raman spectroscopy confirm the construction of the DLC (Diamond Like Carbon) phase in the microstructure of the coatings. The thin coatings synthesized at higher N2/Ar ratios show more increased amount of sp 3 hybridization, improved wettability, higher internal stress, and enhanced mechanical properties, i.e., higher hardness. However, these are accompanied by lower antibacterial performance. Plastic hardness (H) value of the thin coatings increased from about 2 GPa to 13 GPa by increasing N2/Ar ratio. However, bacterial reduction percent of the thin coatings decreased from 100 to 65% as N2/Ar ratio increased. The resultant outcomes reveal the critical role of the N2/Ar ratio on tailoring the antibacterial properties of Cu: a-C: N thin coatings as well as mechanical ones.
https://pccc.icrc.ac.ir/article_81746_8cf8089e8668e0e031f61cd319b94fdf.pdf
2021-11-01
281
291
10.30509/pccc.2021.166770.1102
Cu: amorphous-C: N
Thin coating
Magnetron sputtering
Surface properties
Antibacterial
Mechanical properties
S.
Khamseh
khamseh-sa@icrc.ac.ir
1
Department of Nanomaterials and Nanocoatings, Institute for Color Science and Technology (ICST), Tehran, Iran
LEAD_AUTHOR
M.
Ganjaee Sari
mo-ganjae@icrc.ac.ir
2
Department of Nanomaterials and Nanocoatings, Institute for Color Science and Technology (ICST), Tehran, Iran
AUTHOR
E.
Alibakhshi
eiman-alibakhshi@yahoo.com
3
Surface Coatings and Corrosion Department, Institute for Color Science and Technology (ICST),Tehran, Iran
AUTHOR
M.
Nemati
nemati-m@yahoo.com
4
Department of Nanomaterials and Nanocoatings, Institute for Color Science and Technology (ICST), Tehran, Iran
AUTHOR
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51
ORIGINAL_ARTICLE
Microwave Assisted Green Isolation of Laccaic Acid from Lac Insect (Kerria lacca) for Wool Dyeing
The utilization of sustainable products in the applied field is the recent demand of the global community. In this work the colouring behavior of laccaic acid as a source of natural red dye obtained from lac insect has been studied for the dyeing of wool fabric under microwave treatment. The extract was prepared in acidic medium and stimulated through MW treatment up to 7 min and used to dye fabrics. For developing new shades, eco-friendly green mordants such as extracts of acacia and turmeric were employed along with chemical mordants for comparative studies. The obtained results reveal that extract made in acidic medium after exposure for 5 minutes. has given high colour strength onto un-irradiated fabric when employed for 65 minutes at 75 °C. The rating of fastness properties shows that bio-anchors have given good ratings under optimal conditions. It is inferred that this eco-friendly tool has not only increased the coloring yield of natural anthraquinone dye from lac but also the inclusion of bio-mordants has made the natural coloration process more sustainable.
https://pccc.icrc.ac.ir/article_81752_3c2b8aa0faed647fd8ed176fe5acd0f9.pdf
2021-11-01
293
299
10.30509/pccc.2021.166734.1090
Acacia
Lac
Microwave radiation
Sustainability
wool
S.
Adeel
shahidadeel@gcuf.edu.pk
1
Department of Chemistry, Government College University, Faisalabad 38000, Pakistan
LEAD_AUTHOR
F.
Rehman
furminhas@gcuf.edu.pk
2
Department of Applied Chemistry, Government College University, Faisalabad 38000, Pakistan
AUTHOR
M.
Pervaiz
aatccgcufchapter@gmail.com
3
Department of Applied Chemistry, Government College University, Faisalabad 38000, Pakistan
AUTHOR
M.
Hussaan
mhussaan7866@gmail.com
4
Department of Botany, Government College University, Faisalabad 38000, Pakistan
AUTHOR
N.
Amin
nimraamingc@gmail.com
5
Department of Applied Chemistry, Government College University, Faisalabad 38000, Pakistan
AUTHOR
A.
Majeed
aqsamajeed292@gmail.com
6
Department of Applied Chemistry, Government College University, Faisalabad 38000, Pakistan
AUTHOR
H.
Rehman
hamoodr63@yahoo.com
7
Applied Chemistry Research centre, PCSIR Laboratories Complex, Ferozepur Road, Lahore, Pakistan
AUTHOR
S. Herrera-García, M. Aguirre-Ramírez, J. Torres-Pérez, Comparison between Allura Red dye discoloration by activated carbon and azo bacteria strain, Environ. Sci. Pollut. Res., 27(2020), 29688–29696.
1
T. A. Khattab, M. S. Abdelrahman, M. Rehan, Textile dyeing industry: environmental impacts and remediation, Environ. Sci. Pollut. Res., 27(2020), 3803-3818.
2
A. Sharma, S. Kadam, P. Mathur, J. Sheikh, Re-using henna natural dyeing wastewater for colouration and multifunctional finishing of linen fabric, Sustain. Chem. Pharm., 11(2019), 17-22.
3
A. Haji, Application of D‐optimal design in the analysis and modelling of dyeing of plasma‐treated wool with three natural dyes, Colour. Technol., 136(2020), 137-146.
4
A. Haji, Dyeing of cotton fabric with natural dyes improved by mordants treatment, Prog. Color Colorants Coat., 12(2019), 191-201.
5
T. Agnhage, A. Perwuelz, N. Behary, Towards sustainable Rubiatinctorum L. dyeing of woven fabric: How life cycle assessment can contribute, J. Clean. Prod., 141(2017), 1221-1230.
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N. Amin, S. Adeel, T. Ahamd, M. Muneer, A. Haji, Sustainable application of cochineal-based anthraquinone dye for the coloration of bio-mordanted silk fabric, Environ. Sci. Pollut. Res., 27(2020), 6851-6860.
7
P. M. D. S. Silva, T. R. Fiaschitello, R. S. de-Queiroz, H. S. Freeman, S. A. da-Costa, P. Leo, S. M. da Costa, Natural dye from Croton UrucuranaBaill. bark: Extraction, physicochemical characterization, textile dyeing and colour fastness properties, Dyes Pigm., 173(2020), 107953.
8
M. Hosseinnezhad, K. Gharanjig, R. Jafari, H. Imani, Green dyeing of Woolen Yarns with weld and Madder natural dyes in the presences of Biomordant, Prog. Color Colorants Coat.,14(2020), 35-45.
9
S. Tambi, A. Mangal, N. Singh, J. Sheikh, Cleaner production of dyed and functional polyester using natural dyes vis-a-vis exploration of secondary shades, Prog. Color Colorants Coat., 14(2020), 121-128.
10
S. Adeel, N. Habib, S. Arif, F. U. Rehman, M. Azeem, F. Batool, N. Amin, Microwave-assisted eco-dyeing of bio mordanted silk fabric using cinnamon bark (CinnamomumVerum) based yellow natural dye, Sustain. Chem. Pharm., 17(2020), 100306.
11
M. Hosseinnezhad, K. Gharanjig, R. Jafari, H. Imani, N. Razani, Cleaner colorant extraction and environmentally wool dyeing using oak as eco-friendly mordant, Environ. Sci. Pollut. Res., 47(2020), 1-12.
12
S. Adeel, S. Kiran, N. Habib, A. Hassan, S. Kamal, M. A. Qayyum, K. Tariq, Sustainable ultrasonic dyeing of wool using coconut coir extract, Text. Res. J., 90(2020), 744-756.
13
A. Sutlović, I. Brlek, V. Ljubić, M. I. Glogar, Optimization of dyeing process of cotton fabric with cochineal dye, Fibers Polym. 21(2020), 555-563.
14
Serrano, A. V. D. Doel, M. van Bommel, J. Hallett, I. Joosten, K. J. van den Berg, Investigation of crimson-dyed fibres for a new approach on the characterization of cochineal and kermes dyes in historical textiles, Anal. Chim. Acta, 897(2015), 116-127.
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R. Mongkholrattanasit, C. Saiwan, N. Rungruangkitkrai, N. Punrattanasin, K. Sriharuksa, C. Klaichoi, M. Nakpathom, Ecological dyeing of silk fabric with lac dye by using padding techniques, J. Text. Inst., 106(2015), 1106-1114.
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A. Raman, Discovery of Kerria lacca (Insecta: Hemiptera: Coccoidea), the lac insect, in India in the late 18th century, Curr. Sci., 106(2014), 886.
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M. M. Kamel, R. M. El-Shishtawy, B. M. Yussef, H. Mashaly, Ultrasonic assisted dyeing: III. Dyeing of wool with lac as a natural dye, Dyes Pigm., 65(2005), 103-110.
18
L. V. Haule, L. Nambela, Q, Mgani, A review on source, chemistry, green synthesis and application of textile colorants, J. Clean. Prod., 246(2020), 119036.
19
M. Zuber, S. Adeel, F. U. Rehman, F. Anjum, M. Muneer, M. Abdullah, K. M. Zia, Influence of microwave radiation on dyeing of bio-mordanted silk fabric using neem bark (Azadirachtaindica)-based tannin natural dye, J. Nat. Fibers, 17(2020),1410-1422.
20
M. Hussaan, M. N. Iqbal, S. Adeel, M. Azeem, M. T. Javed, A. Raza, Microwave-assisted enhancement of milkweed (Calotropis procera L.) leaves as an eco-friendly source of natural colorants for textile, Environ. Sci. Pollut. Res., 24(2017), 5089-5094.
21
Q. W. Zhang, L. G. Lin, W. C. Ye, Techniques for extraction and isolation of natural products: a comprehensive review, Chin. Med., 17(2018), 13-20.
22
S. Adeel, M. Hussaan, F. U. Rehman, N. Habib, M. Salman, S. Naz, N. Akhtar, Microwave-assisted sustainable dyeing of wool fabric using cochineal-based carminic acid as natural colorant, J. Nat. Fibers, 19(2019), 1026-1034.
23
K. Sinha, S. Chowdhury, P. D. Saha, S. Datta, Modeling of microwave-assisted extraction of natural dye from seeds of Bixaorellana (Annatto) using response surface methodology (RSM) and artificial neural network (ANN), Ind. Crops Prod., 41(2013), 165-171.
24
S. Adeel, K. Naseer, S. Javed, S. Mahmmod, R. C. Tang, N. Amin, S. Naz, Microwave-assisted improvement in dyeing behavior of chemical and bio-mordanted silk fabric using safflower (Carthamustinctorius L) extract, J. Nat. Fibers, 17(2020), 55-65.
25
S. A. Rabia, H. P. Mazhar, B. A. Samad, A. A. Alvira, An efficient ultrasonic and microwave assisted extraction of organic Henna dye for dyeing of synthetic polyester fabric for superior colour strength properties, Ind. Text., 70(2019), 303-308.
26
S. Adeel, M. Salman, S. A. Bukhari, K. Kareem, A. Hassan, M. Zuber, Eco-friendly food products as source of natural colourant for wool yarn dyeing, J. Nat. Fibers,17(2020), 635-649.
27
Q. Zhou, L. J. Rather, A. Ali, W. Wang, Y. Zhang, Q. M. R. Haque, Q. Li, Environmental friendly bioactive finishing of wool textiles using the tannin-rich extracts of Chinese tallow (Sapiumsebiferum L.) waste/fallen leaves, Dyes Pigm., 176(2020), 108230.
28
M. Shabbir, L. J. Rather, M. Azam, Q. M. R. Haque, M. A. Khan, F. Mohammad, Antibacterial functionalization and simultaneous coloration of wool fiber with the application of plant-based dyes, J. Nat. Fibers, 17(2020), 437-449.
29
N. Rani, L. Jajpura, B. S. Butola, Ecological Dyeing of Protein Fabrics with Carica papaya L. Leaf Natural Extract in the Presence of Bio-mordants as an Alternative Copartner to Metal Mordants, J. Inst. Eng. India Ser. E., 101(2020), 19-31.
30
K. Phan, V. D. Broeck, V. Speybroeck, K. De Clerck, K. Raes, S. De Meester, The potential of anthocyanins from blueberries as a natural dye for cotton: A combined experimental and theoretical study, Dyes Pigm., 176(2020), 108180.
31
D. S. Silva, P. M. Fiaschitello, T. R. de Queiroz, R. S. Freeman, H. S. da Costa, S. A. Leo, P. da Costa, Natural dye from Croton urucuranaBaill. bark: Extraction, physicochemical characterization, textile dyeing and color fastness properties, Dyes Pigm., 173 (2020), 107953.
32
A. Haji, Dyeing of cotton fabric with natural dyes improved by mordants and plasma treatment, Prog. Color Colorants Coat., 12(2019), 191-201.
33
S. Kiran, A. Hassan, S. Adeel, M. A. Qayyum, M. S. Yousaf, M. Abdullah, N. Habib, Green dyeing of microwave treated silk using coconut Coir based tannin natural dye, Ind. Text., 71(2020), 227-234
34
ORIGINAL_ARTICLE
Carbon Surfaces Doped with (Co3O4-Cr2O3) Nanocomposite for High-Temperature Photo Thermal Solar Energy Conversion Via Spectrally Selective Surfaces
Invention new thin films nano-coating to obtain high-level performance spectrally selective surfaces to enhance solar energy by spin and casting methods, thin films coating are deposited by these techniques on aluminum and glass substrates that were pre-cleaned. Nanocomposite thin film coating comprising (Co3O4:Cr2O3) and carbon to gain an economical coating. The coating has a high absorptivity of solar energy. Nanomaterials have been used in various concentration ratios to dope carbon, and Energy Dispersive Analysis (EDX) was used to determine carbon ash's chemical composition; SEM measured its practical size. Optical properties have been studied by the UV-Visible Spectra and reflectivity tests in a range from 250-1300 nm at room temperature. Absorbance coefficient, transmittance, reflectance, skin depth, optical density, optical energy gap (Eg), and Urbach energy of nanocomposite thin films have also been specified. The Eg of doped C has been measured with different concentration ratios of (Co3O4:Cr2O3) such as sample F (0.5:2.5/7), sample G (1:2/7), sample H (1.5:1.5/7), the sample I (2:1/7), and sample K (2.5:0.5/7) wt. %, the concentration of C is fixed for all samples (7) wt. %. The results revealed that the Eg is ranged (2.9-3.9 eV) and the absorptivity in the ranged (88-93.2 %) for all doped samples. The absorptivity values of nanocomposites are very close to semiconductor elements, which have high absorptivity to the wavelength intensity. The synthesized coating will be used over a flat plate collector as a trap to absorb solar energy for a highly feasible selective surface.
https://pccc.icrc.ac.ir/article_81750_e5e01d34d9fc99c9228fecb358b0b5b1.pdf
2021-11-01
301
315
10.30509/pccc.2021.166749.1098
Cobalt oxide
Chromium oxide
Optical properties
Energy band gap
absorptivity
R. N.
Abed
rasheednema@yahoo.com
1
Mechanical Engineering Department, Engineering College, Al-Nahrain University, Jadriah, Baghdad, Iraq.
LEAD_AUTHOR
A. R. N.
Abed
abdulrahman.n.abed@ced.nahrainuniv.edu.iq
2
Mechanical Engineering Department, Engineering College, Al-Nahrain University, Jadriah, Baghdad, Iraq.
AUTHOR
E.
Yousif
emad_yousif@hotmail.com
3
Department of Chemistry, College of Science, Al-Nahrain University, Jadriah, Baghdad, Iraq
AUTHOR
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